Reduction of niobium pentoxide by carbon

dc.contributor.author Stevens, Ernest
dc.contributor.author Wilhelm, H.
dc.contributor.department Ames National Laboratory
dc.date 2018-02-13T16:18:52.000
dc.date.accessioned 2020-06-29T23:20:06Z
dc.date.available 2020-06-29T23:20:06Z
dc.date.embargo 2013-10-24
dc.date.issued 1961-02-01
dc.description.abstract <p>The investigations of the reduction of niobium pentoxide by carbon showed that niobium metal could be prepared by a direct reduction. High temperatures in the region of 2000°C but below the melting point of niobium and dynamic vacuum of one micron or less were the principal experimental conditions employed throughout the course of this study. The reaction, which followed very closely the stoichiometry of the equation Nb2o5 +5C ---> 2Nb + 5CO, began at a temperature near 1200°C and was nearly completed at 1600°C. The data indicated that it might be possible to allow reduction to take place at approximately 1800°C. After the reaction is completed at this temperature, raising of the temperature of the reaction material to nearly 2000°C might eliminate residual oxygen as a result of volatilization of a lower oxide of niobium.</p>
dc.format.mimetype application/pdf
dc.identifier archive/lib.dr.iastate.edu/ameslab_isreports/45/
dc.identifier.articleid 1044
dc.identifier.contextkey 4761922
dc.identifier.s3bucket isulib-bepress-aws-west
dc.identifier.submissionpath ameslab_isreports/45
dc.identifier.uri https://dr.lib.iastate.edu/handle/20.500.12876/6952
dc.language.iso en
dc.relation.ispartofseries IS-339
dc.source.bitstream archive/lib.dr.iastate.edu/ameslab_isreports/45/17_01_00_06_AmesLab_IS_0339_o.pdf|||Sat Jan 15 00:19:43 UTC 2022
dc.subject.disciplines Metallurgy
dc.title Reduction of niobium pentoxide by carbon
dc.type article
dc.type.genre report
dspace.entity.type Publication
relation.isOrgUnitOfPublication 25913818-6714-4be5-89a6-f70c8facdf7e
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