Single-crystal X-ray diffraction and resonant X-ray magnetic scattering at helium-3 temperatures in high magnetic fields at beamline P09 at PETRA III
dc.contributor.author | Francoual, S. | |
dc.contributor.author | Strempfer, J. | |
dc.contributor.author | Liu, Yong | |
dc.contributor.author | Skaugen, A. | |
dc.contributor.author | Canfield, Paul | |
dc.contributor.author | Poli, S. | |
dc.contributor.author | Blume, J. | |
dc.contributor.author | Wolff-Fabris, J. | |
dc.contributor.author | Lograsso, Thomas | |
dc.contributor.department | Ames National Laboratory | |
dc.contributor.department | Physics and Astronomy | |
dc.contributor.department | Materials Science and Engineering | |
dc.contributor.department | Ames Laboratory | |
dc.date | 2018-05-27T05:38:25.000 | |
dc.date.accessioned | 2020-06-29T23:27:31Z | |
dc.date.available | 2020-06-29T23:27:31Z | |
dc.date.copyright | Thu Jan 01 00:00:00 UTC 2015 | |
dc.date.issued | 2015-01-01 | |
dc.description.abstract | <p>The resonant scattering and diffraction beamline P09 at PETRA III at DESY is equipped with a 14 T vertical field split-pair magnet. A helium-3 refrigerator is available that can be fitted inside the magnet's variable-temperature insert. Here the results of a series of experiments aimed at determining the beam conditions permitting operations with the He-3 insert are presented. By measuring the tetragonal-to-orthorhombic phase transition occurring at 2.1 K in the Jahn-Teller compound TmVO4, it is found that the photon flux at P09 must be attenuated down to 1.5 × 109 photons s-1 for the sample to remain at temperatures below 800 mK. Despite such a reduction of the incident flux and the subsequent use of a Cu(111) analyzer, the resonant X-ray magnetic scattering signal at the Tm <em>L</em>III absorption edge associated with the spin-density wave in TmNi2B2C below 1.5 K is intense enough to permit a complete study in magnetic field and at sub-Kelvin temperatures to be carried out.</p> | |
dc.description.comments | <p>This article is published as Francoual, S., J. Strempfer, J. Warren, Y. Liu, A. Skaugen, S. Poli, J. Blume, F. Wolff-Fabris, P. C. Canfield, and T. Lograsso. "Single-crystal X-ray diffraction and resonant X-ray magnetic scattering at helium-3 temperatures in high magnetic fields at beamline P09 at PETRA III." <em>Journal of Synchrotron Radiation </em>22, no. 5 (2015): 1207-1214. DOI: <a href="http://dx.doi.org/10.1107/S1600577515014149" target="_blank">10.1107/S1600577515014149</a>. Posted with permission.</p> | |
dc.format.mimetype | application/pdf | |
dc.identifier | archive/lib.dr.iastate.edu/ameslab_pubs/413/ | |
dc.identifier.articleid | 1423 | |
dc.identifier.contextkey | 12204724 | |
dc.identifier.s3bucket | isulib-bepress-aws-west | |
dc.identifier.submissionpath | ameslab_pubs/413 | |
dc.identifier.uri | https://dr.lib.iastate.edu/handle/20.500.12876/7983 | |
dc.language.iso | en | |
dc.source.bitstream | archive/lib.dr.iastate.edu/ameslab_pubs/413/2015_Lograsso_SingleCrystal.pdf|||Sat Jan 15 00:10:44 UTC 2022 | |
dc.source.uri | 10.1107/S1600577515014149 | |
dc.subject.disciplines | Engineering Physics | |
dc.subject.disciplines | Materials Science and Engineering | |
dc.subject.keywords | X-ray diffraction | |
dc.subject.keywords | resonant X-ray magnetic scattering | |
dc.subject.keywords | helium-3 insert cryostat | |
dc.subject.keywords | sub-Kelvin temperatures | |
dc.subject.keywords | X-ray beam heating | |
dc.subject.keywords | single-crystal | |
dc.title | Single-crystal X-ray diffraction and resonant X-ray magnetic scattering at helium-3 temperatures in high magnetic fields at beamline P09 at PETRA III | |
dc.type | article | |
dc.type.genre | article | |
dspace.entity.type | Publication | |
relation.isAuthorOfPublication | c5a8128b-7d98-4b8f-92d7-b1385e345713 | |
relation.isAuthorOfPublication | 316ee29f-99a9-49bc-a048-0f43caf97aa5 | |
relation.isOrgUnitOfPublication | 25913818-6714-4be5-89a6-f70c8facdf7e | |
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