Acyl furans from cyclohexane-1,3-diones – A synthesis of hibiscone C

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2019-04-25
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Qu, Yang
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Kraus, George
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Ames National Laboratory

Ames National Laboratory is a government-owned, contractor-operated national laboratory of the U.S. Department of Energy (DOE), operated by and located on the campus of Iowa State University in Ames, Iowa.

For more than 70 years, the Ames National Laboratory has successfully partnered with Iowa State University, and is unique among the 17 DOE laboratories in that it is physically located on the campus of a major research university. Many of the scientists and administrators at the Laboratory also hold faculty positions at the University and the Laboratory has access to both undergraduate and graduate student talent.

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Chemistry

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The Department of Chemistry was founded in 1880.

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1880-present

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A direct route to acyl furans was developed using dithiane anion addition followed by deprotection/aromatization. This led to an efficient synthesis of hibiscone C.

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This is a manuscript of an article published as Qu, Yang, and George A. Kraus. "Acyl furans from cyclohexane-1, 3-diones–A synthesis of hibiscone C." Tetrahedron Letters 60, no. 17 (2019): 1186-1188. DOI: 10.1016/j.tetlet.2019.03.055. Posted with permission.

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Tue Jan 01 00:00:00 UTC 2019
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